Natural Gas Testing (Review, interpret and confirm the accuracy of Hydrocarbon results by GC)

Course Properties

Course date: 03-12-2017
Course End Date: 07-12-2017
Location Dubai

Course Description:

  This course is designed to provide expert gas chromatography testing for petroleum, petroleum refined products, natural gas, LPG gases, petrochemicals, and other chemicals and materials. The course operates hundreds of gas chromatographs in GC labs across different stages of production operations, providing evaluation and interpretation of GC analysis results to achieve high level of accuracy.

 

    The course is designed to complyASTM, ISO, standards and other recognized methods.

   The course includes also the practical maintenance where the important parts of GC aredemonstrated i.e. inject system part, different liner and syringes, maintenance kit,different columns type, TCD, FID, ECD, FPD detectors, and other accessory parts which is variable used.


Who should attend?

   Laboratories chemists and lab technicians in oil fields, power stations, , chemical and petrochemical industries, and in oil refineries,etc.


Curse objectives:

      After completion this course, laboratory managers, staff, and others who might be affected should:

               • To introduce participants to Fundamentals of gas chromatography and how the individual elements interrelate.

               • To be able to competently use methods on a gas chromatograph to produce robust and valid analytical data.

               • To provide a knowledge of gas chromatography operation, maintenance and troubleshooting.

               • To impart the participants advance techniques and knowledge of principles of gasc chromatography.

               • To provide knowledge of accessories and consumables required for gas chromatography operations.

               • To provide good laboratory practices for accurate and reliable analyses.

               • To train participants to know how to change and install gas chromatography parts such as inject systems and columns.

               • To familiarize participants with the techniques used in gas chromatography analysis, qualitative and quantitative

                   methods.


Course outlines:

       Module 1

            What Gas Chromatography Is

               • The System

               • The gas source

               • The inlet

               • The column

               • The detector

               • Data reduction

               • Instrument control

                                Trace levels and ultra-trace detection levels to ppm, ppb, ppt

                                Purity and contamination analysis

                                Component tests and compositional analysis

                                ASTM GC test methods available:

                                                o d1945, d2360, d3710, d3797, d3798, d4420, d4492, d4735, d4815, d5134, d5443, d5599, d5623


                                               o d6293, d6142, d6563, d5580, d6293, d6729, d6729, d6730, d6733, d6839, d6890,
d7423, d7504and

                                                  additional gas chromatography test methods


        Module 2

            Injecting Samples

               • Injection Ports

               • Packed port

               • Split/Splitless port

               • Injection technique

               • Benefits of automatic injection

               • Valves

               • Gas sampling

               • Liquid sampling

               • Inlet Temperature

               • Gas samples

               • Liquid samples

                                Detailed Hydrocarbon Analysis

                                ASTM Chemical Testing

                                Natural Gas Testing

                                Middle Distillates Analysis using 2-dimensional Gas Chromatography

                                Trace Analysis of Petrochemicals and Basic Chemicals

        Module 3

            Separating Components

               • How a Column Separates Components

               • The basic principles of chromatography

               • Column Types

               • Capillary columns

               • Packed columns

               • Column tubing

               • Column Characteristics

               • Column efficiency

               • Gas control

               • Column resolution

               • Column selectivity

               • Capillary or Packed?

               • Column Temperature

               • Isothermal oven

               • Programmed oven

 


        Module 4

            Detecting Components

               • Thermal Conductivity (TCD)

               • How it works

               • Flame Ionization (FID)

               • How it works

               • Electron Capture (ECD)

               • How it works


       Module 5

           Interpreting Chromatograms

               • Peak Measurements

               • Retention time

               • Peak size

               • Integrators and data systems

               • Component Identity

               • Component Amount

               • Uncalibrated calculations

               • Area and height percent

               • Calibrated calculations

               • Normalization

               • External standard

               • Internal standard